在線純水總有機碳分析儀 產(chǎn)品特點
1.儀器采用便攜設(shè)計,使用輕便,方便移動至取樣點。
2.采用嵌入式系統(tǒng),觸摸屏設(shè)計,純中文操作方便簡易。
3.針對制藥用水(TOC含量在1000ppb以下)總有機碳含量的檢測設(shè)計,進(jìn)行檢測。
4.配備大量的儲存空間,能夠存儲大量的測試數(shù)據(jù)。
5.中文打印,輸出測試參數(shù)、測試結(jié)果。
6.在使用、貯存和更換過程中不需要氣體或試劑,無移動部件,減少維修和維護(hù)成本。
7.當(dāng)測試樣品濃度超過規(guī)定限度,儀器能夠自動報警,并輸出控制信號。
8.符合國家2010版《中國藥典》規(guī)定的測試方案,可以提供IQ/OQ/PQ服務(wù)。
在線純水總有機碳分析儀 應(yīng)用領(lǐng)域:
制藥用水(純化水、注射用水)的在線監(jiān)測和實驗室測試,以及清潔驗證;
環(huán)保測試、電子行業(yè)、食品行業(yè)等。
性能規(guī)格:
測量范圍:0.01mg/L~1.000 mg/L(此處可調(diào))
精度:?4%測試范圍
分辨率:0.001mg /L
分析時間:連續(xù)分析
響應(yīng)時間:6分鐘之內(nèi)
檢測極限:0.001mg /L
樣品溫度:1- 95℃
重復(fù)性誤差:≤3%
電源要求/功能:220V
顯示屏:彩色觸摸屏
操作控制:無線藍(lán)牙技術(shù);
儀器各部件的安裝、連接
開箱后,按以下步驟進(jìn)行安裝:
── 根據(jù)裝箱單檢查儀器是否齊備。
── 確定儀器在運輸過程中沒有遭到損壞。
── 拆除機箱的外包裝,將其置于正確位置 。
── 檢查儀器保險絲是否裝好,連接市電電纜到接線端子。
── 根據(jù)安裝圖連接進(jìn)液和出液管路 。
── 系統(tǒng)通電 。
工作原理
本儀器采用紫外氧化的原理,將樣品中的有機物氧化為二氧化碳,二氧化碳的測試采用的是直接電導(dǎo)率法,通過測試經(jīng)過氧化反應(yīng)的樣品的總碳含量和未經(jīng)過氧化反應(yīng)的樣品總無機碳的含量差值來測定總有機碳含量,即:總有機碳(TOC)=總碳(TC)-總無機碳(TIC)。
主要特征:
(1) 高精度、高靈敏度,操作簡單。
(2) 人性化操作界面,有一鍵運行功能,自動管路清洗功能。
(3) 高性能CPU,觸摸屏設(shè)計,超大640*480點陣真彩顯示器。
(4) 不用拆開機箱更換UV燈和泵管。
(5) 檢測上限可設(shè)定,自動上限報警功能。
(6) 具有RS232數(shù)據(jù)接口,歷史數(shù)據(jù)可存儲6個月。
(7) 離線檢測和在線檢測可選配。
(8) 具有打印功能
系統(tǒng)組成
TOC分析儀的組成包括以下7個主要部分:
① 在線檢測裝置(在線型儀器配備)
② 樣品蠕動泵
③ 分流器
④ 氧化反應(yīng)器
⑤ 二氧化碳傳感器
⑥ 微處理控制器和電子線路板
⑦ 輸出接口
分流器
水樣進(jìn)入儀器后分成相同流量的兩路,其中一路通過延遲線圈進(jìn)入二氧化碳傳感器,檢測TIC,另一路通過氧化反應(yīng)器利用紫外燈(UV燈)加二氧化鈦薄膜光催化氧化作用將有機物分解為二氧化碳,進(jìn)入二氧化碳傳感器檢測TC。總有機碳可通過這個差值計算得到:TOC = TC–TIC。
二氧化碳傳感器
儀器上安裝有兩個二氧化碳傳感器,由電導(dǎo)率傳感器和溫度傳感器組成。電導(dǎo)率測量采用雙精度技術(shù),可以實現(xiàn)自動校準(zhǔn)和溫度補償。TIC傳感器用于檢測未經(jīng)氧化的水樣中二氧化碳濃度,同時檢測水樣的電導(dǎo)率值;TC傳感器用于檢測水樣本身含有的二氧化碳和水樣中有機物經(jīng)分解后產(chǎn)生的二氧化碳濃度的總和。
使用與操作方法
開始檢測并計入檢測次數(shù),檢測完畢后顯示最后一次檢測結(jié)果,其中幾次檢測的結(jié)果均自動保存在查詢記錄當(dāng)中。檢測次數(shù)的設(shè)置方式為:用“選擇”鍵移動光標(biāo),用“設(shè)置”鍵修改數(shù)字,按“確定”鍵進(jìn)行確認(rèn),進(jìn)入分析界面。先進(jìn)行四次沖洗過程
環(huán)境要求
儀器應(yīng)在一個恒溫恒濕且適于工作的環(huán)境中進(jìn)行。避免陽光直射和超常溫度;溫度過高(超過104?F,40℃)會導(dǎo)致運行失常,溫度過低(低于50?F,10℃)會導(dǎo)致測量值誤差過大。
注意事項
● 該儀器初始的包裝材料需小心保存,安裝需由本公司的專業(yè)技術(shù)人員進(jìn)行操作。
● 若儀器由于任何原因必須返修,必須將其裝入原紙箱中以防運輸途中損壞。
測試準(zhǔn)備
1)將儀器安放在平穩(wěn)、清潔的操作臺上;
2)準(zhǔn)備好存儲廢液的容器,并且把出液口的管路接到容器中;
3)準(zhǔn)備好待測的樣品液。對于長時間沒有測試的儀器,一定要進(jìn)行管路沖洗,
沖洗時間一般在15 到 30 分鐘左右。
Product features
1. The instrument adopts a portable design, which is lightweight and easy to move to the sampling point.
2. Adopting embedded system and touch screen design, pure Chinese operation is convenient and simple.
3. Design and conduct testing for the total organic carbon content of pharmaceutical water (TOC content below 1000ppb).
4. Equipped with a large amount of storage space, capable of storing a large amount of test data.
5. Print in Chinese, output test parameters and test results.
6. No gas or reagents are required during use, storage, and replacement, and there are no moving parts, reducing repair and maintenance costs.
When the concentration of the test sample exceeds the specified limit, the instrument can automatically alarm and output a control signal.
8. According to the testing plan specified in the 2010 edition of the Chinese Pharmacopoeia, IQ/OQ/PQ services can be provided.
Application field:
Online monitoring and laboratory testing of pharmaceutical water (purified water, injection water), as well as cleaning validation;
Environmental testing, electronics industry, food industry, etc.
Performance specifications:
Measurement range: 0.01mg/L~1.000 mg/L (adjustable here)
Accuracy:?4% Test range
Resolution: 0.001mg/L
Analysis time: continuous analysis
Response time: Within 6 minutes
Detection limit: 0.001mg/L
Sample temperature: 1-95℃
Repeatability error:≤3%
Power requirements/function: 220V
Display screen: Color touch screen
Operation control: wireless Bluetooth technology;
Installation and connection of various components of the instrument
After unpacking, follow the following steps for installation:
Check if the instruments are complete according to the packing list.
Ensure that the instrument has not been damaged during transportation.
Remove the outer packaging of the chassis and place it in the correct position.
Check if the instrument fuse is installed properly and connect the mains cable to the wiring terminal.
Connect the inlet and outlet pipelines according to the installation diagram.
Power on the system.
operational principle
This instrument adopts the principle of ultraviolet oxidation to oxidize organic matter in the sample to carbon dioxide. The measurement of carbon dioxide is carried out using the direct conductivity method. The total organic carbon content is determined by measuring the difference between the total carbon content of the sample that has undergone oxidation reaction and the total inorganic carbon content of the sample that has not undergone oxidation reaction. That is, total organic carbon (TOC)=total carbon (TC) - total inorganic carbon (TIC).
Main features:
(1) High precision, high sensitivity, and simple operation.
(2) Humanized operation interface, with one click operation function and automatic pipeline cleaning function.
(3) High performance CPU, touch screen design, large 640 * 480 dot matrix true color display.
(4) No need to open the chassis to replace the UV lamp and pump tube.
(5) The detection upper limit can be set, with automatic upper limit alarm function.
(6) Equipped with RS232 data interface, historical data can be stored for 6 months.
(7) Offline detection and online detection are optional.
(8) With printing function
system composition
The composition of TOC analyzer includes the following 7 main parts:
①Online detection device (equipped with online instruments)
②Sample peristaltic pump
③Diverter
④Oxidation reactor
⑤Carbon dioxide sensor
⑥Microprocessor controllers and electronic circuit boards
⑦Output interface
Diverter
After entering the instrument, the water sample is divided into two paths with the same flow rate. One path enters the carbon dioxide sensor through a delay coil to detect TIC, while the other path decomposes organic matter into carbon dioxide through the photocatalytic oxidation of titanium dioxide film using a UV lamp in an oxidation reactor, and enters the carbon dioxide sensor to detect TC. The total organic carbon can be calculated by this difference: TOC=TC–TIC.
Carbon dioxide sensor
There are two carbon dioxide sensors installed on the instrument, consisting of conductivity sensors and temperature sensors. The conductivity measurement adopts dual precision technology, which can achieve automatic calibration and temperature compensation. TIC sensors are used to detect the concentration of carbon dioxide in unoxidized water samples, while also detecting the conductivity value of the water samples; The TC sensor is used to detect the total concentration of carbon dioxide contained in the water sample itself and the carbon dioxide produced by the decomposition of organic matter in the water sample.
Usage and operation methods
Start the detection and count the number of detections. After the detection is completed, the last detection result will be displayed, and the results of several detections will be automatically saved in the query record. The way to set the number of detections is to use the "Select" key to move the cursor, use the "Set" key to modify the number, press the "OK" key to confirm, and enter the analysis interface. Perform four flushing processes first
Environmental requirements
The instrument should be operated in a constant temperature, humidity, and suitable working environment. Avoid direct sunlight and abnormal temperatures; Excessive temperature (over 104?F, 40℃) can cause abnormal operation, while low temperature (below 50?F, 10℃) can lead to significant measurement errors.
matters needing attention
The initial packaging material of the instrument needs to be carefully stored, and installation needs to be carried out by our company's professional technical personnel.
If the instrument needs to be repaired for any reason, it must be packed in the original cardboard box to prevent damage during transportation.
Test preparation
1) Place the instrument on a stable and clean operating table;
2) Prepare a container for storing waste liquid and connect the outlet pipeline to the container;
3) Prepare the sample solution for testing. For instruments that have not been tested for a long time, it is necessary to perform pipeline flushing,
The flushing time is generally around 15 to 30 minutes.
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