離線純化水TOC水質分析儀 產品特點
1.儀器采用便攜設計,使用輕便,方便移動至取樣點。
2.采用嵌入式系統,觸摸屏設計,純中文操作方便簡易。
3.針對制藥用水(TOC含量在1000ppb以下)總有機碳含量的檢測設計,進行檢測。
4.配備大量的儲存空間,能夠存儲大量的測試數據。
5.中文打印,輸出測試參數、測試結果。
6.在使用、貯存和更換過程中不需要氣體或試劑,無移動部件,減少維修和維護成本。
7.當測試樣品濃度超過規定限度,儀器能夠自動報警,并輸出控制信號。
8.符合國家《中國藥典》 CP2010規定的測試方案,可以提供IQ/OQ/PQ服務。
離線純化水TOC水質分析儀 氧化反應器
儀器利用UV射線在二氧化鈦光催化劑的作用下將有機化合物氧化成二氧化碳,氧化反應器是一個UV燈外包螺旋形的石英管。UV燈發出185nm和254nm的光線,使水產生光分解。
H2O hν(185nm)(TiO2)? OH? H?
羥基自由基(OH?)能完全把有機化合物氧化為二氧化碳。
有機物 OH?? CO2 H2O
UV燈的使用壽命為6個月,當更換時間到期時儀器將出現警告信息,提醒用戶更換UV燈。
二氧化碳測量循環
儀器每4分鐘檢測得出一個數據(包括TOC值和電導率值),在4分鐘的測量循環中TC和TIC是獨立檢測的。
裝箱清單
試驗主機 | 一臺 | |
采集管 | 兩條 | |
電源線 | 一條 | |
控制系統 | 一套 | |
數據采集系統 | 一套 | |
產品使用說明書 | 一份 | |
產品合格證、保修卡 | 一份 |
測定原理:儀器采用紫外氧化的原理,將水溶液中的總有機碳氧化為二氧化碳,并且測定其含量,二氧化碳的測試采用的是直接電導率法,通過測試經過氧化反應的水溶液總碳含量和未經過氧化反應的樣品總無機碳的含量差值來測定總有機碳含量,即:總有機碳(TOC)=總碳(TC)-總無機碳(TIC)。
TOC就是關于進行改進和如何最好的實施這些改進的一套管理理念和管理原則,可以幫助企業識別出在實現目標的過程中存在著哪些制約因素——TOC稱之為“約束”,并進一步指出如何實施必要的改進來一一消除這些約束,從而更有效的實現企業目標。
Product Features
1. The instrument adopts a portable design, which is easy to use and convenient to move to the sampling point.
2. Adopting an embedded system and touch screen design, pure Chinese operation is convenient and easy.
3. Design and conduct testing for the total organic carbon content of pharmaceutical water (TOC content below 1000ppb).
4. Equipped with a large amount of storage space, capable of storing a large amount of test data.
5. Print in Chinese and output test parameters and results.
6. No gas or reagents are required during use, storage, and replacement, and there are no moving parts, reducing maintenance and repair costs.
When the concentration of the test sample exceeds the specified limit, the instrument can automatically sound an alarm and output a control signal.
8. According to the testing plan specified in the Chinese Pharmacopoeia CP2010, IQ/OQ/PQ services can be provided.
Oxidation reactor
The instrument uses UV rays to oxidize organic compounds into carbon dioxide under the action of titanium dioxide photocatalyst. The oxidation reactor is a spiral quartz tube wrapped around a UV lamp. The UV lamp emits light at 185nm and 254nm to decompose aquatic products.
H2O hν(185nm)(TiO2)OH? H?
Hydroxyl radicals (OH?) can completely oxidize organic compounds to carbon dioxide.
Organic compounds OH?CO2 H2O
The service life of UV lamps is 6 months. When the replacement time expires, the instrument will display a warning message to remind the user to replace the UV lamp.
Carbon dioxide measurement cycle
The instrument detects data (including TOC and conductivity values) every 4 minutes, and TC and TIC are independently detected during the 4-minute measurement cycle.
Packing List
One experimental host
Two collection tubes
One power cord
One set of control system
A set of data collection system
One copy of the product user manual
One copy of product qualification certificate and warranty card
Measurement principle: The instrument adopts the principle of ultraviolet oxidation to oxidize the total organic carbon in the aqueous solution to carbon dioxide and determine its content. The carbon dioxide test adopts the direct conductivity method, which determines the total organic carbon content by testing the difference between the total carbon content of the oxidized aqueous solution and the total inorganic carbon content of the sample without oxidation reaction, that is, total organic carbon (TOC)=total carbon (TC) - total inorganic carbon (TIC).
TOC is a set of management concepts and principles about making improvements and how to best implement them. It can help companies identify the constraints that exist in the process of achieving their goals, which TOC refers to as "constraints", and further point out how to implement necessary improvements to eliminate these constraints one by one, in order to more effectively achieve their corporate goals.
廢水的性質或水質是水和各種雜質組成的復雜體系所表現出來的綜合特性,這種特性在工程實...急性毒性的單位通常是以在特定暴露時間內使試驗生物死亡50%的毒物或廢水濃度,即半致死濃度LD50來表示。
從理論上對化工污水TOC與COD_a的相關性進行了分析,對在實際工作中測得的TOC和COD_a數據進行了回歸分析。結果表明,化工污水的TOC和COD_a之間有著良好的相關性。在一定條件下,利用回歸方程可以從測得的TOC值推算出COD_a值,或者從COD_a值推算出TOC值。因此,TOC值可以用來表示有機廢水的污染程度,也可做為有機污染物的一個控制指標。
有很好的相關性[Z,31一、前言在同一廢水樣中,如無其它干擾,且氧化完全,則測得的TOC值與COD值成正比例關系,長期以來,評價水體中有機物朽染的程度即COD—KTOC。因C Oz—CO卜所以*一都是利用經典方法測定COD和BOD。BOD/五32/12=2.667。
應用范圍
該儀器可用于檢測制藥工業中純化水、注射用水和去離子水中有機碳的濃度;也可用于半導體行業中超純水TOC的檢測。
在制藥領域和生物化學領域清潔驗證過程中,可用于驗證清潔效果。
該儀器具有在線檢測功能,可以在線監測制藥工業的制水系統、半導體工業的超純水制備系統和晶片工藝過程、電廠去離子水制備過程等。
離線檢測
離線檢測時,儀器可從樣品瓶或其它沒有壓力的容器直接取樣。儀器管路沖洗和儀器校準應在離線狀態操作。若樣品中有不可溶性微粒,應經過濾膜(孔徑60μm或更小)過濾后進入儀器,以防止樣品中的微粒阻塞儀器。儀器的進樣管為1/16英寸的Teflon管,經蠕動泵抽進管路中的水樣流速約為0.5 ml/min。
主要技術參數
電 源:220V?22V
電源頻率:50Hz?1Hz
額定功率:100W
基本尺寸:44cm?18cm?26cm
檢測極限:0.001mg/L
檢測精度:?5%
檢測范圍:0.001mg/L~1.000mg/L
分析時間:4min
響應時間:15 min以內
樣品溫度:1-95℃
環境溫度:10-40℃ 溫度變化在?5℃/d以內
內部樣品流速:0.5 ml/min
相對濕度:≤ 85%
重復性誤差:≤ 3%
零點漂移:?5%
量程漂移:?5%
The nature or quality of wastewater is a comprehensive characteristic exhibited by a complex system composed of water and various impurities, which is important in engineering practice The unit of acute toxicity is usually expressed as the half lethal concentration (LD50) of the toxic substance or wastewater that causes 50% death of the test organism within a specific exposure time.
Theoretical analysis was conducted on the correlation between TOC and COD_a in chemical wastewater, and regression analysis was performed on the TOC and COD_a data measured in practical work. The results indicate a good correlation between TOC and COD_a in chemical wastewater. Under certain conditions, the COD_a value can be calculated from the measured TOC value using regression equations, or the TOC value can be calculated from the COD_a value. Therefore, TOC value can be used to indicate the degree of pollution in organic wastewater and can also be used as a control indicator for organic pollutants.
There is a good correlation [Z, 31]. Preface: In the same wastewater sample, if there is no other interference and the oxidation is complete, the measured TOC value is directly proportional to the COD value. For a long time, the degree of organic matter decay in water bodies has been evaluated as COD-KTOC. Since C Oz-CO is calculated, the classic methods are used to determine COD and BOD. BOD/5-32/12=2.667.
Application scope
This instrument can be used to detect the concentration of organic carbon in purified water, injection water, and deionized water in the pharmaceutical industry; It can also be used for the detection of TOC in ultrapure water in the semiconductor industry.
In the pharmaceutical and biochemical fields, it can be used to verify the cleaning effect during the cleaning validation process.
This instrument has online detection function, which can monitor the water production system in the pharmaceutical industry, the ultrapure water preparation system and chip process in the semiconductor industry, and the deionized water preparation process in power plants online.
Offline detection
When conducting offline testing, the instrument can directly sample from sample bottles or other containers without pressure. Instrument pipeline flushing and instrument calibration should be operated offline. If there are insoluble particles in the sample, they should be filtered through a filter membrane (with a pore size of 60μm or smaller) before entering the instrument to prevent particles from blocking the instrument. The injection tube of the instrument is a 1/16 inch Teflon tube, and the flow rate of the water sample drawn into the pipeline by a peristaltic pump is about 0.5 ml/min.
Main technical parameters
Power supply: 220V?22V
Power frequency: 50Hz?1Hz
Rated power: 100W
Basic dimensions: 44cm?18cm?26cm
Detection limit: 0.001mg/L
Detection accuracy:?5%
Detection range: 0.001mg/L to 1.000mg/L
Analysis time: 4 minutes
Response time: within 15 minutes
Sample temperature: 1-95℃
Environmental temperature: 10-40℃Temperature variation within?5℃/d
Internal sample flow rate: 0.5 ml/min
Relative humidity:≤85%
Repetitive error:≤3%
Zero drift:?5%
Range drift:?5%
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